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关注:1 2013-05-23 12:21

求翻译:取水杨醛5.2 mL(50 mmol)、 50 mL 90%醋酸,5 mL聚乙二醇-400,依顺序加入100 mL圆底烧瓶中,再将27.4 g(50 mmol)硝酸铈铵溶于30 mL水中,加入烧瓶中,水浴加热,维持温度在45-50 ℃,展开剂TLC跟踪,反应约1.5小时。将反应后的混合溶液倒入盛有100 g冰和100 mL水的400 mL烧杯中,静置一天。即析出3-硝基水杨醛和5-硝基水杨醛混合物。是什么意思?

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取水杨醛5.2 mL(50 mmol)、 50 mL 90%醋酸,5 mL聚乙二醇-400,依顺序加入100 mL圆底烧瓶中,再将27.4 g(50 mmol)硝酸铈铵溶于30 mL水中,加入烧瓶中,水浴加热,维持温度在45-50 ℃,展开剂TLC跟踪,反应约1.5小时。将反应后的混合溶液倒入盛有100 g冰和100 mL水的400 mL烧杯中,静置一天。即析出3-硝基水杨醛和5-硝基水杨醛混合物。
问题补充:

  • 匿名
2013-05-23 12:21:38
Water Salicylaldehyde 5.2 mL (50 mmol), 50 mL 90% acetic acid, 5 mL polyethylene glycol -400, according to the order by adding 100 mL round bottom flask, then 27.4 g (50 mmol) dissolved in 30 mL cerium ammonium nitrate water, adding flask, heated in water bath to maintain temperature at 45-50 ℃, the
  • 匿名
2013-05-23 12:23:18
正在翻译,请等待...
  • 匿名
2013-05-23 12:24:58
Takes salicylic aldehyde 5.2 mL (50 mmol), 50 mL 90% acetic acid, 5 mL polyethylene glycol - 400, join in 100 mL round flasks according to the order, again (50 mmol) the ceric dissolves 27.4 g in 30 mL water, joins in the flask, heating in water bath, maintenance temperature in 45-50 ℃, developing s
  • 匿名
2013-05-23 12:26:38
Preparation of salicylaldehyde 5.2 mL (50 mmol), 50 mL 90% acetic acid, 5 mL polyethylene glycol 400, in order to join in a 100 mL round-bottomed flask, then 27.4 g (50 mmol) ammonium ceric nitrate dissolved in 30 mL of water, joining the flask in the water bath heating, maintenance temperature 45-5
  • 匿名
2013-05-23 12:28:18
Salicylidene 5.2 mL intake (50 mmol), 90% 50 mL acetic acid 5 mL polyethylene glycol-400, consecutively joined in 100 mL round bottom flasks, and 27.4 g (50 mmol) ammonium ceric nitrate dissolved in 30 mL water, added to flask in water bath heating to maintain temperature 45-50 ℃, developing agent T
 
 
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